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Standard Capillaries

Standard Capillaries

XPDF uses bespoke capillaries which interface easily with the beamline sample holders. They come in two main varieties: 

Borosilicate Capillaries

Borosilicate is a cheap and easy to work glass which should be used for all cases except those that require temperatures > 500°C. 

Chemical FormulaSi0.798B0.221Al0.023Na0.066K0.006O2 (Schott Duran Data Sheet)
Density2.23 g·cm-3
Outer DiameterInner DiameterWall thicknessLengthVolumefilled mass* with ρ = 1 g·cm-3
1.0 mm0.78 mm0.11 mm40 mm~ 19 ÎĵL~ 9.5 mg
1.5 mm1.17 mm0.165 mm40 mm~ 43 ÎĵL~ 21.5 mg
2.0 mm1.56 mm0.22 mm40 mm~ 76 ÎĵL~ 38.0 mg

Silica Capillaries

Sometimes called "fused quartz" or incorrectly just "quartz", silica has a significantly higher working temperature so can be used for studies > 500°C. We also have some smaller capillaries for very absorbing samples.

Chemical FormulaSiO2 (Fused Quartz Data Sheet)
Density2.203 g·cm-3
Outer DiameterInner DiameterWall thicknessLengthVolumefilled mass* with ρ = 1 g·cm-3
0.4 mm0.3 mm0.05 mm50 mm~ 3.5 ÎĵL~ 1.8 mg
1.0 mm0.8 mm0.1 mm50 mm~ 25 ÎĵL~ 12.5 mg
1.5 mm1.3 mm0.1 mm50 mm~ 66 ÎĵL~ 33 mg
2.5 mm2.3 mm0.1 mm50 mm~ 208 ÎĵL~ 104 mg


*Assumed packing fraction of 0.5


Outer Diameter

Inner Diameter

Wall thickness

Length

Description 

1/8" (3.178 mm)2.90 mm0.139 mm75 mm One end sealed
1/8" (3.200 mm)2.89 mm0.155 mm75 mm Straight through
1/16" (1.578 mm)1.36 mm0.110 mm60 mm  Straight through
1/16" (1.578 mm)1.36 mm0.110 mm60 mm One end sealed

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